Effect of microwave assisted solvothermal process parameters on carbon dioxide adsorption properties of microporous carbon materials

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dc.contributor.authorStaciwa, Piotrpl_PL
dc.contributor.authorSibera, Danielpl_PL
dc.contributor.authorPełech, Iwonapl_PL
dc.contributor.authorNarkiewicz, Urszulapl_PL
dc.contributor.authorLojkowski, Witoldpl_PL
dc.contributor.authorDąbrowska, Sylwiapl_PL
dc.contributor.authorCormia, Roberten
dc.contributor.organizationZachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydział Technologii i Inżynierii Chemicznejpl_PL
dc.contributor.organizationDepartment of Chemical and Environment Engineering, Faculty of Chemical Technology and Engineering, West Pomeranian University of Technology in Szczecinen
dc.contributor.organizationZachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydział Technologii i Inżynierii Chemicznejpl_PL
dc.contributor.organizationDepartment of Chemical and Environment Engineering, Faculty of Chemical Technology and Engineering, West Pomeranian University of Technology in Szczecinpl_PL
dc.contributor.organizationFaculty of Civil and Environmental Engineering, West Pomeranian University of Technology in Szczecinpl_PL
dc.contributor.organizationZachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydział Technologii i Inżynierii Chemicznejpl_PL
dc.contributor.organizationDepartment of Chemical and Environment Engineering, Faculty of Chemical Technology and Engineering, West Pomeranian University of Technology in Szczecinen
dc.contributor.organizationZachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydział Technologii i Inżynierii Chemicznejpl_PL
dc.contributor.organizationDepartment of Chemical and Environment Engineering, Faculty of Chemical Technology and Engineering, West Pomeranian University of Technology in Szczecinen
dc.contributor.organizationInstytut Wysokich Ciśnień Polskiej Akademii Naukpl_PL
dc.contributor.organizationInstitute of High Pressure Physics, Polish Academy of Scienceen
dc.contributor.organizationPolitechnika Warszawska. Wydział Inżynierii Materiałowejpl_PL
dc.contributor.organizationFaculty of Materials Science and Engineering, Warsaw University of Technologyen
dc.contributor.organizationChemistry Faculty, Chemistry Department, Foothill Collegeen
dc.date.accessioned2023-06-28T12:05:44Z
dc.date.available2023-06-28T12:05:44Z
dc.date.issued2020-08-02
dc.description.abstractIn this work, production and characterization of carbon spheres from resorcinol and formaldehyde, using a microwave assisted solvothermal reactor, is presented. The influence of different experimental conditions, e.g., reaction time, pressure, and power, on the structure of the obtained materials, and carbon dioxide adsorption properties, was studied. Using the method described in this work, it is possible to significantly reduce the reaction time, to as low as 10 min, compared with widely described processes carried out in autoclaves, requiring several hours. Simultaneously, it was discovered that the application of higher reactor pressures, over 3 MPa, resulted in the destruction of spherical shape and the formation of graphitic layers. The importance of micropores below 0.4 nm, for adsorption of carbon dioxide, was also shown in this work. Microporous carbon spheres with efficient CO2 adsorption properties (nearly 7 mmol/g at 1 bar and 0 ◦C) were synthesized using this process.en
dc.description.sponsorshipNarodowe Centrum Naukipl_PL
dc.embargo.terms2025-07-01
dc.identifier.citationStaciwa P., et al. (2020). Effect of microwave assisted solvothermal process parameters on carbon dioxide adsorption properties of microporous carbon materials. Microporous and Mesoporous Materials. doi 10.1016/j.micromeso.2020.110829.en
dc.identifier.doi10.1016/j.micromeso.2020.110829
dc.identifier.project2019/33/B/ST8/02044pl_PL
dc.identifier.urihttps://hdl.handle.net/20.500.12539/1798
dc.language.isoplpl_PL
dc.publisherElsevieren
dc.rightsWszelkie prawa zastrzeżonepl_PL
dc.subjectmicroporous carbon spheresen
dc.subjectsolvothermal process parametersen
dc.subjectcarbon dioxide adsorptionen
dc.subject.otherDyscyplina::Nauki inżynieryjno-techniczne::Inżynieria chemicznapl_PL
dc.titleEffect of microwave assisted solvothermal process parameters on carbon dioxide adsorption properties of microporous carbon materialsen
dc.typeArticleen

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